HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 86595355, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | HCID 21901780 | HCID 21901780 | — |
| Product | HCID 86595355 | HCID 86595355 | — |
Reaction Steps
16.8 g (0.07 mol) of 2-chloromethyl-1-(4-nitrophenyl)pyrrolidine (1), 17.2 g (0.21 mol) of methylimidazole and 70 ml of toluene were refluxed for 9 hours. The solvent was evaporated off and the product was recrystallized from isopropanol and then dried under vacuum. 3 g of yellow crystals (2) were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132543B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-638fa5ddce4e489ea4fa24a0c49d2e8e |
| Source note | uspto-grants-2006_11 |