HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromohexanoyl chloride → 8-(6-Bromohexanoyl)-1,2,5,6-tetrahydro-4H-pyrrolo[3,2,1-ij]quinolin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromohexanoyl chloride | HCID 89848 | — |
| Reactant | Pyroquilon | HCID 91665 | — |
| Product | 8-(6-Bromohexanoyl)-1,2,5,6-tetrahydro-4H-pyrrolo[3,2,1-ij]quinolin-4-one | HCID 21887546 | — |
Reaction Steps
Using 1,2,5,6-tetrahydro-4H-pyrrolo[3,2,1-ij]quinolin-4-one (3.00 g) and 6-bromohexanoyl chloride (2.91 ml) according to the same method as that of Reference Example 1, the title compound (3.94 g) was obtained as white crystals having a melting point of 97 to 98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132547B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-ee17a0b4ca974eec9ac18cfea639179a |
| Source note | uspto-grants-2006_11 |