HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 21889441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Silver(II) oxide | HCID 92152 | — |
| Reactant | 3-Nitro-2,4,6-tri(propan-2-yl)benzene-1-sulfonic acid | HCID 21889420 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21889441 | HCID 21889441 | — |
Reaction Steps
Into a flask was charged 20 parts by 2,4,6-triisopropyl-3-nitrobenzenesulfonic acid, 80 parts of acetonitrile and 40 parts of acetone, and the mixture was stirred at room temperature for 16 hours. To this was added 7.46 parts of silver oxide and the mixture was stirred for 16 hours at room temperature. The resulting mixture was filtrated and concentrated to obtain 23.68 parts of silver 2,4,6-triisopropyl-3-nitrobenzenesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135268B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-b6723cc8ef694f04952780b5ed70cd0d |
| Source note | uspto-grants-2006_11 |