HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 21891668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 1-(Bromomethyl)-2,3-difluoro-benzene | HCID 517984 | — |
| Product | HCID 21891668 | HCID 21891668 | — |
Reaction Steps
Preparation takes place in analogy to that described in Example 1 A from 2.74 g (54.75 mmol) of hydrazine hydrate and 3.02 g (14.60 mmol) of 2,3-difluorobenzyl bromide. For work up, the residue is purified by flash chromatography (mobile phase: dichloromethane:methanol 30:1–10:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135474B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-ca5266b8025c473c8b407e460e678a9f |
| Source note | uspto-grants-2006_11 |