Acrylonitrile → HCID 10448103, compound

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The title compound was prepared from 6-methyl-1-phenacyl-quinolinium bromide (103 mg, 0.300 mmol), tetrapyridinecobalt(II) dichromate (193 mg, 0.317 mmol), sodium bicarbonate (63.4 mg, 0.755 mmol), acrylonitrile (100 μL, 1.52 mmol), and N,N-dimethylformamide (2.0 mL), similar to Example 1b, and yielded 40.2 mg (43%) as a yellow solid. 1H NMR (CDCl3): 8.06 (m, 2H), 7.98 (d, J=8.76 Hz, 1H), 7.62–7.71 (m, 4H), 7.57 (t, J=7.56 Hz, 2H), 7.42 (m, 2H), 2.51 (s, 3H).

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