Phenacyl bromide → HCID 10044981, compound

Participants

Reaction Steps

3-Bromo-1-phenacyl-quinolinium bromide: The title compound was prepared from 2-bromo-1-phenyl-ethanone (485 mg, 2.44 mmol), 7-methyl-quinoline (430 mg, 2.07 mmol) and acetonitrile (5 mL), similar to Example 1a, and yielded 303 mg (36%) as a light tan solid: 1H NMR (CD3OD) 9.73 (d, J=2.1 Hz, 1H), 9.65 (d, J=1.8 Hz, 1H), 8.44 (dd, J=1.2, 8.1 Hz, 1H), 8.31–8.18 (m, 4H), 8.08 (m, 1H), 7.81 (m, 1H), 6.67 (m, 2H), 6.91 (s, 2H).

Provenance & Evidence