HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-chloropyridine → HCID 131726056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-chloropyridine | HCID 2734414 | — |
| Reactant | rel-1,1-Dimethylethyl (3aR,6aS)-hexahydro-4-oxocyclopenta[c]pyrrole-2(1H)-carboxylate | HCID 29948688 | — |
| Product | HCID 131726056 | HCID 131726056 | 51% |
Reaction Steps
5-Bromo-2-chloropyridine (1.82 g, 9.46 mmol) and the product from Example 44A (1.64 g, 7.28 mmol) were processed as described in Example 1E to afford the title compound (1.25 g, 51%). MS (DCI/NH3) m/z 339, 341 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135484B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-80ad559ef03945658b15798c061b31e5 |
| Source note | uspto-grants-2006_11 |