HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanal → (5R)-5-ethyl-9-fluoro-5-hydroxy-12-pentyl-4,5,13,15-tetrahydro-1H,3H-oxepino[3',4':6,7]indolizino[1,2-b]quinoline-3,15-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanal | HCID 6184 | — |
| Reactant | (5R)-5-ethyl-9-fluoro-5-hydroxy-4,5,13,15-tetrahydro-1H,3H-oxepino[3',4':6,7]indolizino[1,2-b]quinoline-3,15-dione | HCID 9929755 | — |
| Product | (5R)-5-ethyl-9-fluoro-5-hydroxy-12-pentyl-4,5,13,15-tetrahydro-1H,3H-oxepino[3',4':6,7]indolizino[1,2-b]quinoline-3,15-dione | HCID 69591007 | — |
Reaction Steps
The product of Example 84 is treated with hexanal according to a procedure similar to Stage 95e in order to produce the expected solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135478B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-e38af49d80e74505a7fa2fffb33be6ac |
| Source note | uspto-grants-2006_11 |