HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Ethyl 2-(2-naphthyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Ethyl 2-naphthylacetate | HCID 256821 | — |
| Reactant | Lithium Hexamethyldisilazide | HCID 2733832 | — |
| Product | Ethyl 2-(2-naphthyl)propanoate | HCID 15676675 | 108.7% |
Reaction Steps
5 g (23 mmol) of ethyl 2-naphthylacetate, 23.3 mL (1.0 M, 23 mmol) of lithium bis (trimethylsilyl) amide, and 1.5 mL (24 mmol) of methyl iodide were reacted as described in Preparation 11 to yield 5.71 g of a dark oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135487B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-b917bd4339f84cdfafad31888f9a2555 |
| Source note | uspto-grants-2006_11 |