HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Benzeneacetyl chloride, 4-bromo-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Benzeneacetic acid, 4-bromo- | HCID 74654 | — |
| Product | Benzeneacetyl chloride, 4-bromo- | HCID 181552 | 100% |
Reaction Steps
A solution of 50.0 g (232 mmol) of 4-bromophenyl-acetic acid in 150 mL of thionyl chloride was stirred at room temperature for 18 hr. The mixture was concentrated in vacuo to afford 54 g (100%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135487B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-525cc79c18714006abd154e6e305e59d |
| Source note | uspto-grants-2006_11 |