HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21893489, compound → HCID 11381315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21893489 | HCID 21893489 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11381315 | HCID 11381315 | 99.4% |
Reaction Steps
A solution of 0.024 g (0.078 mmol) of material from Example 130 and 5 mg 5% palladium on carbon in 5 mL ethyl acetate was degassed three times under a hydrogen balloon and stirred at room temperature for 4 hr. The mixture was filtered and concentrated in vacuo. The residue was recrystallized from ether and hexane to afford 0.024 g (99%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135487B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-50cc79fee2354f38b3aa53142f27556c |
| Source note | uspto-grants-2006_11 |