HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 10051956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 11755954 | HCID 11755954 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 10051956 | HCID 10051956 | — |
Reaction Steps
Prepared by the reaction of 4-[8-(4-acetylamino-benzyl)-1-(2-fluorobenzyl)-2,6-dioxo-1,2,6,7-tetrahydro-purin-3-yl]-butyric acid methyl ester with hydrazine (10 equivalents) in methanol/tetrahydrofuran according to the general procedure of Kramer et al. as described in J. Heterocyclic Chem. 1994, 31, 1439. MS, m/z(M+H)=508.2111.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07135475B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-d53cd8adc15c454ebc7dda692db0d763 |
| Source note | uspto-grants-2006_11 |