HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 720807Generated: October 29, 2026
Methacrylic Acid → HCID 23530362, compound
https://huagongshe.com/reaction/720807
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | 2-{[(Oxiran-2-yl)methoxy]methyl}furan | HCID 94306 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 23530362 | HCID 23530362 | 94.8% |
Reaction Steps
A mixture of methacrylic acid (10 g), furfuryl glycidyl ether (15 g) and triethylaminc (0.3 g) was heated to 100° C. for 2 hours then to 105° C. for an additional 2 hours. GC analysis showed 96% conversion. The mixture was taken up into ether, washed with water, followed by saturated sodium bicarbonate, dried with MgSO4 filtered and rotary evaporated to provide 23.7 g of a faintly yellow oil (94.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07135595B2 |
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| Source dataset | uspto-grants-2006_11 |
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| ORD ID | ord-9eb8f8ae35924426a5cc0cf5808122a7 |
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| Source note | uspto-grants-2006_11 |
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