Ammonia → HCID 21895619, compound

HRID 720832Notes

Reaction equation

HRID 720832 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([CH2:8][S:9](Cl)(=[O:11])=[O:10])[CH:5]=[CH:6][CH:7]=1.[NH3:13]>>[I:1][C:2]1[CH:3]=[C:4]([CH2:8][S:9]([NH2:13])(=[O:11])=[O:10])[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 222AmmoniaHCID 15118080HCID 15118080, compound

Product 1

HCID 21895619HCID 21895619, compound

Procedure

A stirred solution of (3-iodophenyl)methanesulfonyl chloride (1 g) in TKF (20 ml) was treated with 0.88 ammonia (25 ml) at room temperature for 30 min. The solvent was removed under reduced pressure and the residue was triturated in ether to give the title compound (0.35 g).

Workup

  1. customThe solvent was removed under reduced pressure
  2. customthe residue was triturated in ether

Sources & evidence

ORD record
ord-36041ef98134422bae12853ef2385745
Source dataset
uspto-grants-2006_11
Patent number
US07135600B2

Reaction notes

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