HRID72188

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC1(C)OB(c2ccc([N+](=O)[O-])cc2)OC1(C)C

HCID2773555

4,4,5,5-tetramethyl-2-(4-nitrophenyl)-1,3,2-dioxaborolane

C12H16BNO4

结构：CCNC(=O)Nc1ccc(-c2nc(N3CCOC[C@@H]3C)c3c(cnn3C)n2)cc1

HCID51039139

未命名化合物

PRODUCTS

生成物

结构：C[C@H]1COCCN1c1nc(-c2ccc([N+](=O)[O-])cc2)nc2cnn(C)c12

HCID58222489

未命名化合物

PROCEDURE

实验过程

This compound was prepared in an analogous fashion to (S)-1-ethyl-3-(4-(1-methyl-7-(3-methylmorpholino)-1H-pyrazolo[4,3-d]pyrimidin-5-yl)phenyl)urea, using 4-nitrophenylboronic acid pinacol ester as the starting material. 1H NMR (CDCl3, 400 MHz) δ ppm 8.62 (d, J=9.0 Hz, 2H), 8.32 (d, J=9.0 Hz, 2H), 8.22 (s, 1H), 4.27 to 4.17 (m, 4H), 4.08 to 3.95 (m, 2H), 3.93 to 3.82 (m, 1H), 3.79 to 3.67 (m, 2H), 3.60 to 3.50 (m, 1H), 1.38 (d, J=6.6 Hz, 3H).