Dimethyl-[1-(3-methyl-4-nitrophenyl)pyrrolidin-3-yl]amine → [1-(4-Amino-3-methylphenyl)pyrrolidin-3-yl]dimethylamine

Participants

Reaction Steps

A suspension of dimethyl-[1-(3-methyl-4-nitrophenyl)pyrrolidin-3-yl]amine (200 mg) and palladium (10% on carbon, 10 mg) in methanol (10 mL) was vigorously stirred under an atmosphere of hydrogen at atmospheric pressure for 5 hours. The catalyst was then filtered off with suction and the filtrate was concentrated. The product with the molecular weight of 219.33 (C13H21N3) was obtained in this way; MS (ESI): 220 (M+H+).

Provenance & Evidence