HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrogen → HCID 69287425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | 2-Pyridinecarboxaldehyde | HCID 14273 | — |
| Reactant | 2-Amino-4-methyl-3-nitropyridine | HCID 243166 | — |
| Product | HCID 69287425 | HCID 69287425 | 49.9% |
Reaction Steps
Similarly to Example N2, the condensation of 2.58 g of 2-amino-4-methyl-3-nitropyridine and 1.8 g of pyridine-2-carbaldehyde gives 2.03 g of the title compound of m.p. 161–163° C. The mass spectrum shows the molecular peak MH+ at 243.0 Da.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138399B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-26c22b8b40cb4f6f908db7c707221a90 |
| Source note | uspto-grants-2006_11 |