4-(4-Methyl-1,4-diazepan-1-yl)aniline → HCID 24859572, compound

HRID 72218Notes

Reaction equation

HRID 72218 reaction equation
CO[C:3]([C:5]1[S:6][C:7]([C:15]([CH:17]2[CH2:22][CH2:21][O:20][CH2:19][CH2:18]2)=[O:16])=[CH:8][C:9]=1[N:10]=[CH:11][N:12]([CH3:14])C)=[O:4].[CH3:23][N:24]1[CH2:30][CH2:29][CH2:28][N:27]([C:31]2[CH:36]=[CH:35]C(N)=[CH:33][CH:32]=2)[CH2:26][CH2:25]1>>[CH3:23][N:24]1[CH2:30][CH2:29][CH2:28][N:27]([C:31]2[CH:36]=[CH:35][C:14]([N:12]3[C:3](=[O:4])[C:5]4[S:6][C:7]([C:15]([CH:17]5[CH2:18][CH2:19][O:20][CH2:21][CH2:22]5)=[O:16])=[CH:8][C:9]=4[N:10]=[CH:11]3)=[CH:33][CH:32]=2)[CH2:26][CH2:25]1

Participants

3

Reactant 2

HCID 130079514-(4-Methyl-1,4-diazepan-1-yl)anilineHCID 68978518HCID 68978518, compound

Product 1

HCID 24859572HCID 24859572, compound

Procedure

3-(Dimethylaminomethyleneamino)-5-(tetrahydropyran-4-carbonyl)thiophene-2-carboxylic acid methyl ester and 4-(4-methyl[1,4]diazepan-1-yl)phenylamine were reacted by method A1. The product with the molecular weight of 452.58 (C24H28N4O3S) was obtained in this way; MS (EST): 453 (M+H+).

Workup

  1. customThe product with the molecular weight of 452.58 (C24H28N4O3S) was obtained in this way

Sources & evidence

ORD record
ord-d798952d9805410b8ae68d9d7cdf0662
Source dataset
uspto-grants-2014_09
Patent number
US08828991B2

Reaction notes

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