Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thioacetamide | HCID 2723949 | — |
| Reactant | 3-Methoxy-4-nitrobenzohydrazide | HCID 21883875 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178488187 | HCID 178488187 | — |
Reaction Steps
The mixture consisting of 590 mg g of 3-methoxy-4-nitrobenzoic hydrazide, 6 ml of pyridine and 210 mg of thioacetamide was heated to 95° C. for 2 hours. After cooling, the volatile fractions were removed under reduced pressure at 40° C. and the residue was subjected to column chromatography purification (silica gel, solvent: 95:5 dichloromethane:methanol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07138414B2 |
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| Source dataset | uspto-grants-2006_11 |
|---|
| ORD ID | ord-1b016a8858ed40a18d46df865caf42b4 |
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| Source note | uspto-grants-2006_11 |
|---|
