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HRID 722201作成日:2026年10月25日

Benzoyl isocyanate, 2-chloro-4-fluoro- → HCID 178488185、化合物

https://huagongshe.com/reaction/722201

反応式

関与物質

役割名称HCID仕込み量
反応物Benzoyl isocyanate, 2-chloro-4-fluoro-HCID 11521269—
反応物HCID 178488184HCID 178488184—
溶媒AcetonitrileHCID 6342—
生成物HCID 178488185HCID 178488185—

反応手順

The solution of equivalent amounts of 2-chloro-4-fluorobenzoyl isocyanate was added dropwise to the solution of 35 mg of 2-methoxy-4-(5-methyl-4H-[1,2,4]triazol-3-yl)phenylamine in 3 ml of acetonitrile and the mixture was stirred at room temperature for 30 minutes. The solid was then filtered off with suction, stirred with t-butyl methyl ether, filtered off with suction and dried under reduced pressure.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07138414B2
出典データセットuspto-grants-2006_11
ORD IDord-4144f6acc56a4529a02386356894212a
出典メモuspto-grants-2006_11