化工社化工社 化学情報印刷レポート · 研究参考用
Benzoyl isocyanate, 2-chloro-4-fluoro- → HCID 178488185、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoyl isocyanate, 2-chloro-4-fluoro- | HCID 11521269 | — |
| 反応物 | HCID 178488184 | HCID 178488184 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | HCID 178488185 | HCID 178488185 | — |
反応手順
The solution of equivalent amounts of 2-chloro-4-fluorobenzoyl isocyanate was added dropwise to the solution of 35 mg of 2-methoxy-4-(5-methyl-4H-[1,2,4]triazol-3-yl)phenylamine in 3 ml of acetonitrile and the mixture was stirred at room temperature for 30 minutes. The solid was then filtered off with suction, stirred with t-butyl methyl ether, filtered off with suction and dried under reduced pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07138414B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-4144f6acc56a4529a02386356894212a |
| 出典メモ | uspto-grants-2006_11 |