4-(4-Methyl-1,4-diazepan-1-yl)aniline → HCID 86628970, compound

HRID 72236Notes

Reaction equation

HRID 72236 reaction equation
CO[C:3]([C:5]1[S:6][C:7]([CH:15]=[O:16])=[CH:8][C:9]=1[N:10]=[CH:11][N:12]([CH3:14])C)=[O:4].[CH3:17][N:18]1[CH2:24][CH2:23][CH2:22][N:21]([C:25]2[CH:30]=[CH:29]C(N)=[CH:27][CH:26]=2)[CH2:20][CH2:19]1>>[CH3:17][N:18]1[CH2:24][CH2:23][CH2:22][N:21]([C:25]2[CH:30]=[CH:29][C:14]([N:12]3[C:3](=[O:4])[C:5]4[S:6][C:7]([CH:15]=[O:16])=[CH:8][C:9]=4[N:10]=[CH:11]3)=[CH:27][CH:26]=2)[CH2:20][CH2:19]1

Participants

3

Reactant 2

HCID 130079514-(4-Methyl-1,4-diazepan-1-yl)anilineHCID 57618749HCID 57618749, compound

Product 1

HCID 86628970HCID 86628970, compound

Procedure

3-(Dimethylaminomethyleneamino)-5-formylthiophene-2-carboxylic acid methyl ester was reacted with 4-(4-methylperhydro-1,4-diazepin-1-yl)phenylamine by method A1. The product with the molecular weight of 368.46 (C19H20N4O2S) was obtained in this way; MS (ESI): 369 (M+H+).

Workup

  1. customThe product with the molecular weight of 368.46 (C19H20N4O2S) was obtained in this way

Sources & evidence

ORD record
ord-97384abf195b4fe1b4f47eaf875eef7b
Source dataset
uspto-grants-2014_09
Patent number
US08828991B2

Reaction notes

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