2-Amino-4-chlorophenol → HCID 10084758, compound

Participants

Reaction Steps

Prepared by the method of Example 1a), from 4-chloro-2-aminophenol (429 mg, 2.9 mmol) and 4-methoxy-3-aminobenzoic acid (500 mg, 2.9 mmol) the subtitle compound was obtained, 111 mg (10%). 1H NMR (CDCl3) δ 7.70(d, J=1.9 Hz, 1H), 7.65(dd, J=1.9, 8.3 Hz, 1H), 7.59(d, J=1.9 Hz, 1H), 7.46(d, J=8.3 Hz, 1H), 7.28(dd, J=1.9, 8.3 Hz, 1H), 6.90(d, J=8.3 Hz, 1H), 3.96(s, 3H). MS 275 m/z (M+H)+.

Provenance & Evidence