HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium ethoxide → 2-(5-Nitro-2-ethoxyphenyl)-5-phenylbenzoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | 2-(2-Fluoro-5-nitrophenyl)-5-phenylbenzoxazole | HCID 21884334 | — |
| Product | 2-(5-Nitro-2-ethoxyphenyl)-5-phenylbenzoxazole | HCID 21884572 | — |
Reaction Steps
Prepared by the method of Example 40a), from 2-(5-nitro-2-fluorophenyl)-5-phenylbenzoxazole (200 mg, 0.60 mmol) and sodium ethoxide (41 mg, 0.61 mmol) the subtitle compound was obtained (197 mg, 91%). 1H NMR (DMSO) δ 8.92(d, 1H), 8.51(dd, 1H), 8.18(s, 1H), 7.95(d, 1H), 7.83(d, 2H), 7.56(t, 3H), 7.47(t, 3H), 4.50(q, 2H), 1.57(t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-ef2930e60d9c4601802f454f0e231626 |
| Source note | uspto-grants-2006_11 |