Pentylamine → 2-(5-Nitro-2-pentylaminophenyl)-5-phenylbenzoxazole

HRID 722551Notes

Reaction equation

HRID 722551 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][C:3]=1[C:11]1[O:12][C:13]2[CH:19]=[CH:18][C:17]([C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)=[CH:16][C:14]=2[N:15]=1.[CH2:26]([NH2:31])[CH2:27][CH2:28][CH2:29][CH3:30]>>[N+:8]([C:5]1[CH:6]=[CH:7][C:2]([NH:31][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])=[C:3]([C:11]2[O:12][C:13]3[CH:19]=[CH:18][C:17]([C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)=[CH:16][C:14]=3[N:15]=2)[CH:4]=1)([O-:10])=[O:9]

Participants

3

Reactant 2

HCID 8060PentylamineHCID 218843342-(2-Fluoro-5-nitrophenyl)-5-phenylbenzoxazole

Product 1

HCID 218844842-(5-Nitro-2-pentylaminophenyl)-5-phenylbenzoxazole

Procedure

Prepared by the method of Example 54a), from 2-(2-fluoro-5-nitrophenyl)-5-phenylbenzoxazole (200 mg, 0.60 mmol), and pentylamine (2 ml) the subtitle compound was obtained (289 mg, 100%). MS 402 m/z (M+H)+.

Sources & evidence

ORD record
ord-ace8c1c477e8420781d21f649c66741c
Source dataset
uspto-grants-2006_11
Patent number
US07138425B2

Reaction notes

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