p-Toluenesulfonic acid monohydrate → HCID 21884352, compound

Participants

Reaction Steps

Prepared by the method of Example 15c), from N-phenyl-2-fluoro-5-nitrobenzamide (2.89 g, 10.4 mmol) and p-toluenesulfonic acid monohydrate (3.80 g, 20.0 mmol) the subtitle compound was obtained (2.41 g, 90%). 1H NMR (DMSO) δ 8.95(m, 1H), 8.52(m, 1H), 7.90(m, 2H), 7.81(t, 1H), 7.50(m, 2H).

Provenance & Evidence