HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 21884302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 21884435 | HCID 21884435 | — |
| Product | HCID 21884302 | HCID 21884302 | — |
Reaction Steps
Prepared by the method of Example 15b), from N-(2-hydroxy-4-methylphenyl)-2-fluoro-5-nitrobenzamide (300 mg, 2.8 mmol) and p-toluenesulfonic acid monohydrate (1.17 g, 6.16 mmol) the subtitle compound was obtained (403 mg, 53%). MS m/z 273.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-0850d52ba2e642eaa7abba3fb2f4ec81 |
| Source note | uspto-grants-2006_11 |