2-Amino-4-phenylphenol → N-(5-Phenyl-2-hydroxyphenyl)-3-nitro-4-chlorobenzamide

HRID 722621노트

반응식

HRID 722621 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[Cl:13])[C:7](Cl)=[O:8])([O-:3])=[O:2].[C:14]1([C:20]2[CH:25]=[CH:24][C:23]([OH:26])=[C:22]([NH2:27])[CH:21]=2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[C:14]1([C:20]2[CH:25]=[CH:24][C:23]([OH:26])=[C:22]([NH:27][C:7](=[O:8])[C:6]3[CH:10]=[CH:11][C:12]([Cl:13])=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=3)[CH:21]=2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

참가 물질

3

반응물 2

HCID 145622-Amino-4-phenylphenolHCID 1234774-Chloro-3-nitrobenzoyl chloride

생성물 1

HCID 21884357N-(5-Phenyl-2-hydroxyphenyl)-3-nitro-4-chlorobenzamide

실험 절차

Prepared by the method of Example 15b), from 3-nitro-4-chlorobenzoyl chloride (5.28 g, 24.0 mmol) and 4-phenyl-2-aminophenol (3.92 g, 21.0 mmol) the subtitle compound was obtained. The product was used directly in the next step without purification.

출처 및 근거

ORD 기록
ord-2e063dd27fdb45d28ef0a9ed24f333dc
출처 데이터셋
uspto-grants-2006_11
특허 번호
US07138425B2

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