HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Nitro-6-propylaminophenyl)-5-(3-methyl-4-chlorophenyl)benzoxazole → 2-(3-Amino-6-propylaminophenyl)-5-(3-methyl-4-chlorophenyl)benzoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Nitro-6-propylaminophenyl)-5-(3-methyl-4-chlorophenyl)benzoxazole | HCID 21884356 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | 2-(3-Amino-6-propylaminophenyl)-5-(3-methyl-4-chlorophenyl)benzoxazole | HCID 21884472 | — |
Reaction Steps
Prepared by the method of Example 47b), from 2-(3-nitro-6-propylaminophenyl)-5-(3-methyl-4-chlorophenyl)benzoxazole (230 mg, 0.48 mmol) and zinc (314 mg, 4.8 mmol) the subtitle compound was obtained (187 mg, 100%). MS 392.3 m/z (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-9d880b7c8b0d43e8805ebcd7783e793f |
| Source note | uspto-grants-2006_11 |