HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenylboronic acid → 2-(3-Nitro-6-propylaminophenyl)-5-(4-chlorophenyl)benzoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenylboronic acid | HCID 74299 | — |
| Reactant | 2-(5-bromo-1,3-benzoxazol-2-yl)-4-nitro-N-propylaniline | HCID 5303802 | — |
| Product | 2-(3-Nitro-6-propylaminophenyl)-5-(4-chlorophenyl)benzoxazole | HCID 21884340 | — |
Reaction Steps
Prepared by the method of Example 15d), from 2-(3-nitro-6-propylaminophenyl)-5-bromobenzoxazole (400 mg, 1.59 mmol) and 4-chlorophenylboronic acid (258 mg, 1.65 mmol) the subtitle compound was obtained (284 mg, 64%). MS 408.2 m/z (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138425B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-1e2939fccae340ce870c3c6a667a02d3 |
| Source note | uspto-grants-2006_11 |