HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromododecane → (2S,3R)-2-(N,N-Dibenzylamino)-3-pentadecanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromododecane | HCID 8919 | — |
| Reactant | (S)-2-Dibenzylamino-propionaldehyde | HCID 11107860 | — |
| Product | (2S,3R)-2-(N,N-Dibenzylamino)-3-pentadecanol | HCID 58743395 | — |
Reaction Steps
According to the method of Example 26, from aldehyde 4 (273 mg, 1.08 mmol) and 1-bromododecane (671 mg, 2.69 mmol), alcohol 31 was obtained as a colorless oil (195 mg, 43% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138547B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-fc36ce42b5d7465ca9d5115322540afc |
| Source note | uspto-grants-2006_11 |