HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromotridecane → (2S,3R)-2-(N,N-Dibenzylamino)-3-hexadecanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromotridecane | HCID 13000 | — |
| Reactant | (S)-2-Dibenzylamino-propionaldehyde | HCID 11107860 | — |
| Product | (2S,3R)-2-(N,N-Dibenzylamino)-3-hexadecanol | HCID 58743369 | — |
Reaction Steps
According to the method of Example 26, from aldehyde 4 (332 mg, 1.31 mmol) and 1-bromotridecane (863 mg, 3.28 mmol), alcohol 33 was obtained as a colorless oil (172 mg, 30% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138547B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-e48867949d73470fb71ea1b25ec5fd34 |
| Source note | uspto-grants-2006_11 |