HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopentadecane → (4S,5R)4-(N,N-Dibenzylamino)-5-eicosanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopentadecane | HCID 12394 | — |
| Reactant | (S)-2-(dibenzylamino)pentanal | HCID 44223341 | — |
| Product | (4S,5R)4-(N,N-Dibenzylamino)-5-eicosanol | HCID 58743391 | — |
Reaction Steps
According to the method of Example 26, from aldehyde 11 (123 mg, 0.44 mmol) and 1-bromopentadecane (318 mg, 1.09 mmol), alcohol 65 was obtained as a colorless oil (161 mg, 75% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138547B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-7d382c90ffc5416ab555e245fdc9281c |
| Source note | uspto-grants-2006_11 |