HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorovaleryl chloride → 9-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | 1,2,6,7-tetrahydro-5H-pyrido[3,2,1-ij]quinolin-3-one | HCID 13694564 | — |
| Product | 9-(5-chloropentanoyl)-1,2,6,7-tetrahydropyrido[3,2,1-ij]quinolin-3(5H)-one | HCID 21887259 | — |
Reaction Steps
Using 2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one and 5-chlorovaleryl chloride according to the same method as that of Reference Example 1, the title compound (3.53 g) was obtained as colorless crystals having a melting point of 83–84° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138533B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-6aafe6411be646cf932f45dd72fda6c8 |
| Source note | uspto-grants-2006_11 |