6-Bromohexanoyl chloride → HCID 21887179, compound

HRID 722924Notes

Reaction equation

HRID 722924 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][S:10]([CH3:13])(=[O:12])=[O:11].[Br:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20](Cl)=[O:21]>>[Br:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[C:4]([NH:9][S:10]([CH3:13])(=[O:12])=[O:11])[CH:5]=1)=[O:21]

Participants

3

Reactant 2

HCID 898486-Bromohexanoyl chlorideHCID 773523HCID 773523, compound

Product 1

HCID 21887179HCID 21887179, compound

Procedure

Using N-(2-methoxyphenyl)methanesulfonamide (10.0 g) and 6-bromohexanoyl chloride (8.37 ml) according to the same method as that of Reference Example 1, the title compound (9.80 g) was obtained as colorless crystals.

Sources & evidence

ORD record
ord-9fc3f55633684b0d8cbe0b93fbc49f36
Source dataset
uspto-grants-2006_11
Patent number
US07138533B2

Reaction notes

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