HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloropropionyl chloride → HCID 21886810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloropropionyl chloride | HCID 69364 | — |
| Reactant | Pyroquilon | HCID 91665 | — |
| Product | HCID 21886810 | HCID 21886810 | — |
Reaction Steps
Using 1,2,5,6-tetrahydro-4H-pyrrolo[3,2,1-ij]quinolin-4-one (10.0 g) and 3-chloropropanoyl chloride (6.06 ml) according to the same method as that of Reference Example 1, the title compound (12.0 g) was obtained as colorless crystals having a melting point of 154 to 155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138533B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-65dacd2c27ed430891a593be51f66a5e |
| Source note | uspto-grants-2006_11 |