HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one → HCID 21887034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one | HCID 231553 | — |
| Reactant | HCID 21887510 | HCID 21887510 | — |
| Product | HCID 21887034 | HCID 21887034 | 112.2% |
Reaction Steps
Using 484 mg (3 mmol) of 1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one and 850 mg (3.3 mmol) of (±)-5-[[2-(2-chlorophenyl)ethyl](methyl)amino]hexanoic acid obtained in Reference Example 202 according to the same method as that of Example, a free base compound of the title compound (860 mg) was obtained as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07138533B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-308e51e8cc9347ab821f0e356454ea3a |
| Source note | uspto-grants-2006_11 |