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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 722976Generated: October 30, 2026

1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one → HCID 21887034, compound

https://huagongshe.com/reaction/722976

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-oneHCID 231553—
ReactantHCID 21887510HCID 21887510—
ProductHCID 21887034HCID 21887034112.2%

Reaction Steps

Using 484 mg (3 mmol) of 1,3-dimethyl-1,3-dihydro-2H-benzimidazol-2-one and 850 mg (3.3 mmol) of (±)-5-[[2-(2-chlorophenyl)ethyl](methyl)amino]hexanoic acid obtained in Reference Example 202 according to the same method as that of Example, a free base compound of the title compound (860 mg) was obtained as a pale yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07138533B2
Source datasetuspto-grants-2006_11
ORD IDord-308e51e8cc9347ab821f0e356454ea3a
Source noteuspto-grants-2006_11