HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycidyl methacrylate → Butyl Acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycidyl methacrylate | HCID 7837 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Product | Butyl Acrylate | HCID 8846 | — |
Reaction Steps
After the completion of the reaction, the solution was cooled to room temperature. To the solution, 3 g of glycidyl methacrylate, 0.1 g of p-methoxyphenol and 0.3 g of tetrabutylammonium bromide were added. The mixture was stirred until these added compounds dissolved completely. The solution thus obtained was heated to 80° C., and an addition reaction was allowed to take place for 16 hours between the carboxyl group in the copolymer and the epoxy group in the glycidyl methacrylate. Thereafter, the solution was cooled to room temperature to obtain an alkali soluble resin (A-1) in the form of resin solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141355B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-a177d74bdc054399b556193d8553accc |
| Source note | uspto-grants-2006_11 |