N,N,N'-trimethyl-N'-(4-nitrophenyl)-1,2-ethanediamine → N-(2-Dimethylaminoethyl)-N-methylbenzene-1,4-diamine

Participants

Role	Name	HCID	Charge
Reactant	N,N,N'-trimethyl-N'-(4-nitrophenyl)-1,2-ethanediamine	HCID 21873305	—
Catalyst	Zinc	HCID 23994	—
Product	N-(2-Dimethylaminoethyl)-N-methylbenzene-1,4-diamine	HCID 21873395	—

Reaction Steps

The compound was prepared by zinc dust reduction of N,N,N′-trimethyl-N′-(4-nitrophenyl)ethane-1,2-diamine in analogy to the method in example 3. The product with the molecular weight of 193.29 (C11H19N3); MS (ESI): 194 ([M+H]+), was obtained in this way.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07141561B2
Source dataset	uspto-grants-2006_11
ORD ID	ord-31bccd887b124b24bf2f233545e19fbf
Source note	uspto-grants-2006_11