(4-Aminophenoxy)benzene → HCID 21873324, compound

Participants

Reaction Conditions

Reaction Steps

Carbonyldiimidazole (136 mg) was added to a solution of 4-phenoxyaniline (155 mg) in dimethylformamide (3 mL) at 0° C. After 30 minutes, allyl-(4-benzyloxyphenyl)amine (200 mg) was added and the temperature was increased to 80° C. for 2 hours. A further 2 hours at 120° C., the reaction solution was cooled and then purified by preparative HPLC. The product with the molecular weight of 450.54 (C29H26N2O3); MS (ESI): 451 ([M+H]+), was obtained in this way.

Provenance & Evidence