Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Benzyloxyaniline | HCID 22860 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21873301 | HCID 21873301 | — |
Reaction Steps
A mixture of 4-benzyloxyaniline (3.0 g), allyl bromide (1.27 mL), potassium carbonate (4.2 g) and dimethylformamide (15 mL) was heated at 80° C. for 3 hours. After cooling, the reaction solution was filtered and concentrated. The residue was purified by MPLC. The product with the molecular weight of 239.32 (C16H17NO); MS (ESI):240 ([M+H]+), was obtained in this way.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07141561B2 |
|---|
| Source dataset | uspto-grants-2006_11 |
|---|
| ORD ID | ord-d4633e0fcb8045e4ada2f83c7e1797f4 |
|---|
| Source note | uspto-grants-2006_11 |
|---|
