Phosgene → HCID 67136103, compound

Participants

Reaction Steps

Phosgene (20% in toluene; 0.091 mL) was added dropwise to a solution of N-benzylidene-N′-(4-phenoxyphenyl)hydrazine (50 mg) in toluene (1 mL) at 0° C. After 24 hours at room temperature, 4-(2-dimethylaminoethoxy)aniline (31 mg) was added. After two hours, the crystals which had separated out were filtered off with suction. The product with the molecular weight of 494.60 (C30H30N4O3); MS (ESI): 495 ([M+H]+), was obtained in this way.

Provenance & Evidence