HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-Dodecyloxy-2-decyloxy-1-triphenylmethoxypropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-Bromodecane | HCID 8173 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Trityl ether | HCID 12756307 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-Dodecyloxy-2-decyloxy-1-triphenylmethoxypropane | HCID 21873196 | 52% |
Reaction Steps
The trityl ether of Section B (13.5 g, 0.027 mol) was added dropwise to an ice-cooled suspension of sodium hydride (80%, 1.6 g, 0.054 mol) in 150 mL of tetrahydrofuran under nitrogen. After stirring for 2 hours at room temperature, heat was applied (55° C.). 1-Bromodecane (6 g, 0.027 mol) was added dropwise; heating was continued for 6 hours. After cooling for 3 hours, water was added slowly. Diethyl ether (2×100 mL) was added, and the solution washed with 15 percent sodium thiosulfite, water, and brine. After drying over sodium sulfate, the ether was removed, and the residue was chromatographed with a gradient of hexanes:ethyl acetate (100:0 to 20:1) to give 9 g (52%) of a clear liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141557B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-5c0e39e79082412293bd78a986d25ba4 |
| Source note | uspto-grants-2006_11 |