(1S,3S,4S)-4-azido-3-hydroxy-cyclohexanecarboxylic acid amide → HCID 45083256, compound

Participants

Reaction Steps

To (1S,3S,4S)-4-azido-3-hydroxy-cyclohexanecarboxylic acid amide (352c) (760 mg, 4.13 mmol) in MeOH (30 mL) was added Pd/C (10%, 500 mg), and the mixture hydrogenated under atmospheric pressure for 18 h. On completion of reaction the mixture was filtered through Celite®, the filter pad washed with MeOH, and the combined organic solutions concentrated in vacuo to give a white solid in quantitative yield;

Provenance & Evidence