HCID 21877089, compound → HCID 21877076, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:14]=[C:15]([Cl:17])[CH:16]=1)/[CH:5]=[C:6](\[C:10](=[O:13])[CH2:11][CH3:12])/[C:7](=[O:9])[CH3:8].ClC1C=C(C=C(Cl)C=1)/C=C(/C(=O)CC)\C(=O)C>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:14]=[C:15]([Cl:17])[CH:16]=1)[CH2:5][CH:6]([C:10](=[O:13])[CH2:11][CH3:12])[C:7](=[O:9])[CH3:8]Participants
3
Procedure
The title compound was prepared by a similar method to that of Preparation 6 using (3Z)-3-(3,5-dichlorobenzylidene)-2,4-hexanedione and (3E)-3-(3,5-dichlorobenzylidene)-2,4-hexanedione of Preparations 18 and 19 and was obtained as yellow oil (300 mg).
Sources & evidence
- ORD record
- ord-3feb2829dd8944809cb11c03e587061b
- Source dataset
- uspto-grants-2006_11
- Patent number
- US07141585B2
Reaction notes
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