HuagongsheHuagongshe Chemistry Print Report · For research reference only
Norborna-diene → HCID 69365832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Norborna-diene | HCID 18006658 | — |
| Reactant | HCID 91613900 | HCID 91613900 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69365832 | HCID 69365832 | — |
Reaction Steps
(5R)-3-(4-Methylthiophenyl)-5-azidomethyloxazolidin-2-one (1.62 g, 6.14 mM) was dissolved in dioxane (30 ml), treated with norbornadiene (2.98 g, 31.5 mM) and heated under reflux for 6 hours. After removal of the solvent, the residue was dissolved in the minimum of hot ethyl acetate, filtered, cooled, then diluted with isohexane to precipitate the desired product (600 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141583B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-fe0bffb147204490837e7626037995d5 |
| Source note | uspto-grants-2006_11 |