HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoromethanesulfonic acid, lithium salt → HCID 86610082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoromethanesulfonic acid, lithium salt | HCID 3664839 | — |
| Reactant | Methyl (2R)-2-oxiranecarboxylate | HCID 9877347 | — |
| Reactant | 6-amino-4-fluoro-3-isopropyl-1,3-benzoxazol-2(3H)-one | HCID 68489676 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86610082 | HCID 86610082 | — |
Reaction Steps
Prepared from 6-amino-4-fluoro-3-isopropyl-1,3-benzoxazol-2(3H)-one (Step 2, 0.77 g, 3.66 mmol), methyl (2R)-glycidate (0.374 g, 3.66 mmol) and lithium trifluoromethanesulfonate (0.57 g, 3.66 mmol) in acetonitrile (10 ml) according to the method of EXAMPLE 86, Step 8 (0.89 g, 78%); MS for C14H17FN2O5 m/z 313 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141588B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-fb5eb590bec74a94bacda0376685cdca |
| Source note | uspto-grants-2006_11 |