4-Bromo-m-cresol → HCID 21877314, compound

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[2-(4-Bromo-3-methyl-phenoxymethoxy)-ethyl]-trimethyl-silane was prepared in 86% yield from 4-bromo-3-methyl-phenol according to the procedure for [2-(4-bromo-2-methoxy-5-methyl-phenoxymethoxy)-ethyl]-trimethyl-silane. 1H NMR (300 MHz, CDCl3) δ 7.39 (d, 1 H, J=8.7 Hz), 6.93 (d, 1 H, J=2.7 Hz), 6.75 (dd, 1 H, J=8.7, 2.7 Hz), 5.16 (s, 2 H), 3.74 (t, 2 H, J=8.4 Hz), 2.36 (s, 3H), 0.95 (t, 2 H, J=8.4 Hz), 0.01 (s, 9 H). Anal. (C13H21BrO2Si) C, H. Calculated: C, 49.21; H, 6.67. Found: C, 49.33; H, 6.67.

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