Diethyl Ether → HCID 58747082, compound

Participants

Reaction Steps

310 mg (0.55 mmol) 98 was dissolved in a mixture of 1 mL anisol and 4 mL trifluoroacetic acid and was agitated occasionally by swirling for 30 minutes at ambient temperature. 40 mL of cold ether was added, the precipitate was centrifuged, the ether phase was discarded, and the precipitate washed with ether (1×) then was re-precipitated from 5 mL methanol with 40 mL ether and dried to give 377 mg (96%) 99 as bis-TFA salt. MS: 220.61 (M+2H+).

Provenance & Evidence