HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 87611584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 131726120 | HCID 131726120 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 87611584 | HCID 87611584 | — |
Reaction Steps
The compound of Example 9A is dissolved in THF; an aqueous solution of LiOH is added, and the resultant mixture is stirred at ambient temperature for 3 hours. The reaction is quenched by addition of aqueous phosphoric acid (1N), and extracted with ethyl acetate. The crude material is carried forward without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07141559B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-37e698fce01e423fb073d5798b30355e |
| Source note | uspto-grants-2006_11 |