Boc-L-phenylalaninamide → HCID 11712103, compound

HRID 724742Notes

Reaction equation

HRID 724742 reaction equation
[C:1]([O:5][C:6](=[O:19])[NH:7][C@H:8]([C:16](=[O:18])[NH2:17])[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)([CH3:4])([CH3:3])[CH3:2].[C:20]([N:24]1[C:28](=[O:29])[CH:27]=[C:26](Cl)[S:25]1(=[O:32])=[O:31])([CH3:23])([CH3:22])[CH3:21]>>[C:1]([O:5][C:6](=[O:19])[NH:7][C@H:8]([C:16](=[O:18])[NH2:17])[CH2:9][C:10]1[CH:15]=[CH:14][C:13]([C:26]2[S:25](=[O:31])(=[O:32])[N:24]([C:20]([CH3:22])([CH3:21])[CH3:23])[C:28](=[O:29])[CH:27]=2)=[CH:12][CH:11]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 7020416Boc-L-phenylalaninamideHCID 218786382-Tert-butyl-5-chloro-2,3-dihydro-1lambda6,2-thiazole-1,1,3-trione

Product 1

HCID 11712103HCID 11712103, compound

Procedure

This compound was prepared according to the procedure of Example 1.1, Step 4, using (S)-2-phenyl-1-carbamoyl-ethyl-carbamic acid tert-butyl ester and 9-A as the starting materials. LCMS found for C21H29N3O6SNa (M+Na)+: m/z=474.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-a1bc00e3363c43b38449aaec1d78da32
Source dataset
uspto-grants-2006_11
Patent number
US07141596B2

Reaction notes

Loading…